Neutron Diffraction Structures Of Water In Crystalline Hydrates Of Metal Salts

Document Type

Journal Article

Publisher

John Wiley

Faculty

Faculty of Health, Engineering and Science

School

School of Natural Sciences

RAS ID

20616

Comments

Chandler, G. S., Wajrak, M. and Khan, R. N. (2015), Neutron diffraction structures of water in crystalline hydrates of metal salts. Acta Crystallographica Section B, 71: 275–284. doi: 10.1107/S2052520615005387. Available here

Abstract

Neutron diffraction structures of water molecules in crystalline hydrates of metal salts have been collected from the literature up to December 2011. Statistical methods were used to investigate the influence on the water structures of the position and nature of hydrogen bond acceptors and cations coordinated to the water oxygen. For statistical modelling the data were pruned so that only structures with oxygen as hydrogen acceptors, single hydrogen bonds, and no more than two metals or hydrogens coordinated to the water oxygen were included. Multiple linear regression models were fitted with the water OH bond length and bond angle as response variables. Other variables describing the position and nature of the acceptors and ions coordinated to the waters were taken as explanatory variables. These variables were sufficient to give good models for the bond lengths and angles. There were sufficient structures involving coordinated Mg or Cu for a separate statistical modelling to be done for these cases.

DOI

10.1107/S2052520615005387

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